Blogs about: Amine

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MOM protection of amine

To a stirred solution of the amine (0.005 mol) in 15 mL THF at 0 oC was added sodium hydride (60% in mineral oil, 0.0055 mol). A white solid precipitated and hydrogen gas was evolved. Chloromethyl m… more →

PMGB

dream blog 1

perfectsoup wrote 3 months ago: Okay must get this down quickly for it’s disappearing from my head as I write! This morning (l … more →

Tags: Random, Whatever, Seriously, SCCC, test, History class., Dreams

Doctors........who needs 'em? — 3 comments

amineissa wrote 3 months ago: I am sure all of us have been there. You know… the doctor’s office where you sit down and tell … more →

Tags: Introductions, doctors

Voltron homily

catholickermit wrote 4 months ago: MASS - (Fr Santos) — today’s homily mentioned Father’s favorite anime cartoon grow … more →

Tags: Mass homily, TV, Priesthood, St. John Vianney College Seminary, Miami, Seminarian, Archdiocese of Miami, Pre-Theology, Discernment

MOM protection of amine

pmgb wrote 4 months ago: To a stirred solution of the amine (0.005 mol) in 15 mL THF at 0 oC was added sodium hydride (60% … more →

Tags: Alcohols, protection

Macross Frontier

yamslayer wrote 4 months ago: Now that the first season of Gundam 00 has ended, I have begin Macross Frontier another epic mecha … more →

Mono N-methylation — 2 comments

pmgb wrote 5 months ago: To a solution of the primary amine (0.002 mol) in anhydrous ethanol was added paraformaldehyde (0.0 … more →

Deprotection of benzyl group

pmgb wrote 5 months ago: To a stirred suspension of the N-benzyl derivative (x gm, 0.01 mol) and 10% Pd-C (x gm, equal weigh … more →

Tags: deprotection

Deprotection of BOC group

pmgb wrote 5 months ago: To a stirred solution of the N-BOC derivative (0.01 mol) in 25 mL dichloromethane (in a round botto … more →

Tags: deprotection

Selective protection of amines

pmgb wrote 5 months ago: Case 1 (where the amine is nucleophilic, example-piperazine): To a stirred suspension of the amine … more →

Tags: phenols

Amines from nitriles

pmgb wrote 5 months ago: To a stirred solution of alkylmagnesium bromide (2M solution in ether, 0.039 mol) under nitrogen a … more →

Tags: nitriles, Grignards

Mono N-alkylation — 2 comments

pmgb wrote 5 months ago: To a stirred suspension of Cs2CO3 (0.006 mol) in 3 mL DMF was added the representative primary amin … more →

Tags: N-alkylation

N-alkylation

pmgb wrote 5 months ago: To a suspension of the amine HCl salt (0.0437 mol) in 60 mL acetonitrile cooled by an ice-bath was … more →

Tags: N-alkylation


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